N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.
Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.
Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.
Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.
Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.
The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.
This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.
Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.
In addition to its use as a wine sweetener and a paint improver, lead offered even more benefits as a gasoline additive in the form of a compound known as tetraethyl lead.