Sodium phenolate and acetophenone can be obtained by adding sodium hydrate into azeotrope.
共沸物中加入氢氧钠,分离出钠盐和。
Sodium phenolate and acetophenone can be obtained by adding sodium hydrate into azeotrope.
共沸物中加入氢氧钠,分离出钠盐和。
Phenoxyacetophenone could be prepared from potassium phenolate and m bromoacetophenone via Ullmann reaction catalyzed by copper acetate in high yields.
间氧基可由钾与间溴在醋酸铜催下以高产率合成。
The primary synthetic methods of 4-hydroxycoumarin was reviewed starting from phenol, 2-acetylsalicylic acid, methyl salicylate, and o-hydroxyacetophenone respectively.
概述了4-羟基香豆素的合成方法,重点介绍了法,酰水杨酸法,水杨酸甲酯法,邻羟基法。
The phenols were O-alkylated with 100% conversion and 100% selectivities using phenacyl bromide and benzyl bromide as alkylating reagents.
用溴代和溴苄为烷基,以高产率和100%的转率以及100%的选择性得到了的O-烷基产物。
P-hydroxyacetophenone combined with methyl chloroacetate can get a new acetonate.This new acetonate combined with another compound-ethanolamine and get a new schiff base.
由对羟基与氯酸甲酯反应,得到一种,这种再与醇胺反应得到一种新的希夫碱。
Firstly, p-methylacetophenone was obtained in the presence of alchlor as the catalyst, and the optimum condition was 4:1:2 in molar ratio for toluene, acetic anhydride and alchlor with yield of 86.2%.
首先,以甲和酸酐为原料,在催三氯铝存在下合成对甲基,并确定甲,酸酐和三氯铝的最佳摩尔比为4: 1: 2,收率为86.2%。
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