Sodium phenolate and acetophenone can be obtained by adding sodium hydrate into azeotrope.
共沸物中加入氢氧化钠,分离出钠盐和苯乙酮。
Sodium phenolate and acetophenone can be obtained by adding sodium hydrate into azeotrope.
共沸物中加入氢氧化钠,分离出钠盐和苯乙酮。
Phenoxyacetophenone could be prepared from potassium phenolate and m bromoacetophenone via Ullmann reaction catalyzed by copper acetate in high yields.
间苯氧基苯乙酮可由钾与间溴苯乙酮在醋铜催化下以高产率。
The primary synthetic methods of 4-hydroxycoumarin was reviewed starting from phenol, 2-acetylsalicylic acid, methyl salicylate, and o-hydroxyacetophenone respectively.
概述了4-羟基香豆素方法,重点介绍了苯法,乙酰水法,水酯法,邻羟基苯乙酮法。
The phenols were O-alkylated with 100% conversion and 100% selectivities using phenacyl bromide and benzyl bromide as alkylating reagents.
用溴代苯乙酮和溴苄为烷基化试剂,以高产率和100%转化率以及100%选择性得到了O-烷基化产物。
P-hydroxyacetophenone combined with methyl chloroacetate can get a new acetonate.This new acetonate combined with another compound-ethanolamine and get a new schiff base.
由对羟基苯乙酮与氯乙酯反应,得到一种酮,这种酮再与乙醇胺反应得到一种新希夫碱。
Firstly, p-methylacetophenone was obtained in the presence of alchlor as the catalyst, and the optimum condition was 4:1:2 in molar ratio for toluene, acetic anhydride and alchlor with yield of 86.2%.
首先,以苯和乙酐为原料,在催化剂三氯化铝存在下对基苯乙酮,并确定苯,乙酐和三氯化铝最佳摩尔比为4: 1: 2,收率为86.2%。
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