Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘化钐在分子内环化反应中的应。
Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘化钐在分子内环化反应中的应。
Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
甲
氯为原料,经
化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应总收率为8.05%。
Method The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.
方法克拉霉素为起始原料,经水解、乙
化、环碳酸酯化、氧化、脱碳酸酯化、
化、环氨基甲酸酯化和环合等反应合成目标化合物。
This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.
讨论了草酸二乙酯为原料,经过克莱森缩合、环合、氨解反应合成5甲基异唑3甲
胺工艺的改
。
In this paper, the synthesis of 2 - chloranthraquinone and 2 - aminoanthraquinone was studied.It was prepared from phthalic anhydride by acetyiation, hydrolysis and cyclization.
酐和取代
为原料,经过乙
化、水解及环合反应,合成了2-氯蒽醌和2-氨基蒽醌,并对影响收率的工艺条件
行了研究。
Aqueous titanium trichloride promoted intermolecular reductive cyclization of 1,2 -diketone and o-nitroaniline in basic media provides a convenient method for the synthesis of quinoxaline derivatives.
本文研究了三氯化钛水溶液作下,邻硝基
胺与1,2-二酮在碱性介质中分子间的成环反应,提供了一个方便地合成取代喹喔啉类化合物的方法。
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