Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
苯甲酰氯为原料,经酰
,还原,环
等反应
成左旋西替利嗪盐酸盐,反应总收率为8.05%。
(作用)Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
苯甲酰氯为原料,经酰
,还原,环
等反应
成左旋西替利嗪盐酸盐,反应总收率为8.05%。
Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘

分子内环
反应中的应用。
Method The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.
方法
克拉霉素为起始原料,经水解、乙酰
、环
酸酯
、氧
、脱
酸酯
、酰
、环氨基甲酸酯
和环
等反应
成目标

。
N butyl 2 ethoxy thioacridone was prepared from o chloro benzoic acid and p phenetidine by means of Ullman reaction,cyclization,N alkylation and sulfurization.
邻氯苯甲酸和对乙氧基苯胺为原料,经过胺的苯基
、二芳胺的环
、N-烷基
、硫代
反应
成了N-丁基-2-乙氧基硫代吖啶酮。
This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.
讨论了
草酸二乙酯为原料,经过克莱森缩
、环
、氨解反应
成5甲基异唑3甲酰胺工艺的改进。
In this paper, the synthesis of 2 - chloranthraquinone and 2 - aminoanthraquinone was studied.It was prepared from phthalic anhydride by acetyiation, hydrolysis and cyclization.
苯酐和取代苯为原料,经过乙酰
、水解及环
反应,
成了2-氯蒽醌和2-氨基蒽醌,并对影响收率的工艺条件进行了研究。
Aqueous titanium trichloride promoted intermolecular reductive cyclization of 1,2 -diketone and o-nitroaniline in basic media provides a convenient method for the synthesis of quinoxaline derivatives.
本文研究了三氯
钛水溶液作用下,邻硝基苯胺与1,2-二酮
碱性介质中分子间的成环反应,提供了一个方便地
成取代喹喔啉类

的方法。
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