1.The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.
2.The standard deviations were 0.06 and 0.14 for Phoxim and Quintozene repectively,while the coefficients of variation were 1.14% and 1.34%.The average recoveries were 99.5 and 99.2% separately.